Drying, shrinkage and rehydration characteristics of kiwifruits during hot air and microwave drying (Maskan)
Journal of Food Engineering 48 (2001) 177ą182 www.elsevier.com/locate/jfoodeng Drying, shrinkage and rehydration characteristics of kiwifruits during hot air and microwave drying Medeni Maskan Department of Food Engineering, Engineering Faculty, University of Gaziantep, 27310 Gaziantep, Turkey Received 24 March 2000; accepted 11 September 2000 Abstract Hot air, microwave and hot air-microwave drying characteristics of kiwifruits (5:03 0:236 mm thick) were investigated. Drying rates, shrinkage and rehydration capacities of these drying regimes were compared. The drying took place in the falling rate drying period regardless of the drying method. Drying with microwave energy or assisting hot air drying with microwave energy resulted in increased drying rates and substantial shortening of the drying time. Shrinkage of kiwifruits during microwave drying was greater than hot air drying. Less shrinkage was observed at hot air-microwave drying. Microwave dried kiwifruit slices exhibited lower rehydration capacity and faster water absorption rate than the other drying methods studied. Ó 2001 Elsevier Science Ltd. All rights reserved. Keywords: Drying; Kiwifruits; Rehydration; Shrinkage; Air; Microwave 1. Introduction The most common drying method employed for food materials to date was hot air drying. But there are many Longer shelf-life, product diversity and substantial disadvantages of this method. Among these are low en- volume reduction are the reasons for popularity of dried ergy eciency and lengthy drying time during the falling fruits and vegetables, and this could be expanded further rate period. This is mainly caused by rapid reduction of with improvements in product quality and process ap- surface moisture and consequent shrinkage, which often plications. These improvements could increase the cur- results in reduced moisture transfer and, sometimes, re- rent degree of acceptance of dehydrated foods in the duced heat transfer (Feng & Tang, 1998). Several inves- market. tigators of drying have reported that hot air drying, hence Kiwifruits have very short shelf-life because of soft- prolonged exposure to elevated drying temperatures, re- ening and vitamin loss during storage even at refriger- sulted in substantial degradation in quality attributes, ated conditions (O'Connor-Shaw, Roberts, Ford, & such as colour, nutrients, Żavour, texture, severe shrink- Nottingham, 1994; Agar, Massantini, Hess-Pierce, & age, reduction in bulk density and rehydration capacity, Kader, 1999). In order to extend their shelf-life, kiwi- damage to sensory characteristics and solutes migration fruits, like most fresh fruits, need preservation in some from the interior of the food to the surface (Bouraout, form. A growing resistance of consumers to the use of Richard, & Durance, 1994; Yongsawatdigul & chemicals for food preservation and the increasing Gunasekaran, 1996; Feng & Tang, 1998; Maskan, 2000). popularity of high quality fast-dried foods with good In recent years, microwave drying oered an alter- rehydration properties are now leading to a renewed native way to improve the quality of dehydrated prod- interest in drying operations. From a technological ucts. Usually, drying is not induced by dielectric heating point of view, dehydration is often the nal step in an alone, but most microwave drying systems combine industrial food process and determines, to a large extent, microwave and conventional heating. The heating may the nal quality of the product being manufactured take place in separate operations or simultaneously. (Sereno & Medeiros, 1990). Microwave drying, like conventional drying, is caused by water vapour pressure dierences between interior and surface regions which provide a driving force for moisture transfer. It is most eective at product mois- E-mail address: maskan@gantep.edu.tr (M. Maskan). ture contents below 20% (Mudgett, 1989; Giese, 1992). 0260-8774/01/$ - see front matter Ó 2001 Elsevier Science Ltd. All rights reserved. PII: S 0 2 6 0 - 8 7 7 4 ( 0 0 ) 0 0 155- 2 178 M. Maskan / Journal of Food Engineering 48 (2001) 177ą182 Notation V volume of sample (ml) at any time V0 initial volume of sample (ml) Wd weight of dried sample (g) k drying constant (min 1) Wt weight of rehydrated sample (g) at any time MR moisture ratio X moisture content (kg H2O=kg dry solids) at any r2 coecientof determination time S shrinkage Xe equilibrium moisture content (kg H2O=kg dry solids) SE standard error X0 initial moisture content (kg H2O=kg dry solids) t drying time (min) Therefore, essentially for economic reasons, it has been 700 W at 2450 MHz. was used. The oven has the facility suggested that microwave energy should be applied in the to adjust power (wattage) supply and the time of pro- falling rate period or at a low moisture content (where cessing and was tted with a turntable. The hot air conventional drying takes a long time) to nish drying. drying experiments were performed in a pilot plant tray Microwave drying has been used in drying of herbs (Gi- dryer (UOP 8 tray dryer, Armeld, UK). The operation ese, 1992), potato (Bouraout et al., 1994), raisins (Ko- mode of this dryer was explained in detail elsewhere staropoulos & Saravacos, 1995), apple and mushroom (Maskan, 2000). (Funebo & Ohlsson, 1998), diced apples (Feng & Tang, 1998), carrots (Prabhanjan, Ramaswamy, & Raghavan, 2.3. Drying procedure 1995; Litvin, Mannheim, & Miltz, 1998; Lin, Durance, & Scaman, 1998) and banana (Maskan, 2000). (1) Hot air drying. The dryer was operated at Little data currently exists on processing (minimally an air velocity of 1.29 m/s, parallel to the drying surface processing, packaging, storage etc.) of fresh cut kiwi- of the sample, 60C dry bulb and 27C wet bulb tem- fruits to extend the shelf life. Therefore, the objective of peratures. The study was carried out at constant sample this study is the comparison of the microwave, hot air thickness and at constant temperature. Moisture loss and hot air-microwave nish drying methods for the was recorded by a digital balance (Avery Berkel, processing of kiwifruits in respect to drying, shrinkage CC062D10ABAAGA) at 10 min intervals during drying and rehydration characteristics obtained by the three for determination of drying curves. Kiwifruits were drying techniques. dried until equilibrium (no weight change) was reached. (2) Microwave drying. Dierent microwave power intensities (210, 350, and 490 W) were investigated in 2. Materials and methods microwave drying at constant sample thickness of 5.03 mm. It was observed that (our preliminary tests) 2.1. Material charring and sample boiling occurred at 350 and 490 W power. Therefore, only the 210 W power level was Kiwifruits (Actinidia deliciosa) used in this study were chosen in this study. One glass petri dish (7:1 cm purchased from a local market. The whole samples were diameter 1:2 cm deep), containing the sample, was stored at 4 0:5C before they were used in experiments placed at the centre of the oven turntable in the micro- in order to slow down the respiration, physiological and wave cavity during treatment for even absorption of chemical changes (O'Connor-Shaw et al., 1994). The microwave energy. The presence of the turntable was initial moisture content of kiwifruits was found to be necessary to achieve the optimum oven performance and 4.55 kg H2O=kg dry solids. Prior to drying, samples to reduce the levels of reŻected microwaves onto the were taken out of storage, peeled with a sharp vegetable magnetron (Khraisheh, Cooper, & Magee, 1997). The peeler, and cut into 5:03 0:236 mm thick and drying was performed according to a pre-set power and 40 0:812 mm diameter slices with a cutting machine. time schedule. Moisture loss was measured by taking At least ten measurements of the thickness were made at out and weighing the dish on the digital balance peri- dierent points with a dial micrometer; only slices that odically. When the material reached a constant weight, fell within a 5% range of the average thickness were equilibrium moisture content was assumed to be used. All kiwifruits used for drying were from the same reached. Attention was paid to ensure that the sample batch. The equilibrium moisture content was assumed to was not charred. be the nal moisture content of each run. (3) Air followed by a microwave nish drying. Drying was carried out by a combination of hot air-microwave 2.2. Drying equipment techniques. A 5.03 mm thick kiwifruit sample was dried by hot air initially for 135 min, then, dried by microwave A programmable domestic microwave oven (Arcelik (at 210 W). This point corresponds to a moisture con-
ARMD 580, TURKEY), with maximum output of tent of about 1.2 kg water/kg dry solids. It is a critical M. Maskan / Journal of Food Engineering 48 (2001) 177ą182 179 point, because there was a sudden change in colour the eect of drying method on drying rate, shrinkage parameters (results were not shown) up to this point and rehydration of kiwifruits was evaluated. when the samples were dried by microwave alone (for The drying curves of kiwifruits dried by various about 10 min). The objective of using this combined methods are shown in Fig. 1. It is evident from exam- system was to see if hot air pre-drying aects the drying ination of these curves that the drying of kiwifruits by characteristics and maintains the colour quality of ki- microwave is much faster than drying by hot air or hot wifruits. The details of colour change were presented in air-microwave combination. For example, the time to another study (Maskan, 2001). reach about 0.39 kg water/kg dry solids was 24.0, 225.0 The following diusion model (Eq. (1)) was used to and 136.5 min, respectively. In fact, the drying time for describe drying kinetics of kiwifruits rather than using the sample was reduced to about 89% of the hot air Fick's diusion model. The latter model could not be drying time with the microwave drying and about 40% applied because of severe shrinkage in sample dimen- with the hot air-microwave combination drying method. sions during drying. This indicated that the drying time requirement was signicantly reduced as microwave was introduced. X Xe Maskan (2000) found that the hot air-microwave nish MR exp ktą: 1ą X0 Xe drying reduced the convection drying time of bananas by about 64.3%. Similar results were obtained by dif- ferent authors on drying of fruits and vegetables by 2.4. Shrinkage and rehydration capacity various drying techniques. (Bouraout et al., 1994; Prabhanjan et al., 1995; Lin et al., 1998; Funebo & For shrinkage and rehydration studies, similar drying Ohlsson, 1998). These authors explained that the shorter experiments, given in Section 2.3, were conducted sep- drying time under microwave heating conditions could arately using the same microwave, hot air and micro- be due to the additional energy input, rapid heat pene- wave nish drying conditions. Measurement of tration by microwave and forced expulsion of gases. shrinkage and rehydration times were established from Drying rates were calculated as quantity of moisture preliminary assays. removed per unit time per unit dry solids (kg water/kg Volume changes due to sample shrinkage were mea- dry solids/min). The drying rates of kiwifruits were given sured by a water displacement method as described by in Figs. 2 and 3. From an examination of these gures it (Sjoholm & Gekas, 1995). Measurements were made as is obvious that the drying occurred mostly in the falling quickly as possible (less than 30 s) to avoid water uptake rate period (with two periods), regardless of drying by samples. The shrinkage/volume change of the sam- conditions. Although the kiwifruits have high moisture ples was expressed as a bulk shrinkage ratio of sample content, an expected constant rate period was not volume at any time to initial volume observed in the present study. In Fig. 2, the slope of V the second falling rate line was steeper than that of rst S : 2ą V0 falling rate line (moisture content 1:3 kg water=kg dry solids) and hence drying rate decreased rapidly dur- Rehydration experiments were performed by im- ing last stages of drying. Two falling rate periods were mersing a weighed amount of dried samples into hot water at 50C for 50 min. At 10 min intervals the sam- ples were drained over a mesh for 30 s and quickly blotted with the paper towels 4ą5 times gently in order to eliminate the surface water and then reweighed. The rehydration capacity, described as percentage water gain, was calculated from the sample weight dierence before and after the rehydration as follows: Wt Wdą weight gain %ą 100: 3ą Wd 3. Results and discussion When deciding which process conditions produce the best quality dried products, it is necessary to compare drying time and quality parameters. Good quality was dened as fast rehydration capacity, low bulk density, Fig. 1. Typical drying curves for kiwifruit slices (5:03 0:236 mm little shrinkage, and an attractive colour. In this study, thick). 180 M. Maskan / Journal of Food Engineering 48 (2001) 177ą182 high surface temperature, migration of soluble solids to the surface of the sample and build-up of such soluble materials at the surface as the water evaporates (Feng & Tang, 1998). This results in complex physical and chemical changes in the surface layer. Thereafter, sur- face cracking occurs, tissues split and rupture internally forming open structures due to the temperature rise in the sample, so that moisture transfer is allowed with a greater rate from the cracks and an open structure formed (Maskan & Ibanoglu, 1998). One of the reasons for the greater drying rates (steeper slope) in the second falling rate period has been reported by Maskan and Gogus (1998). They stated that it may be due to cell wall
destruction and, therefore, the resistance to moisture diusion decreases within the sample. The pattern of Fig. 2. Drying rate curves for kiwifruits dried by hot air (60C and drying rate curves, examined in this study, for kiwifruits 1.29 m/s). was similar to that reported for apple purees (Moyls, 1981), carrots (Prabhanjan et al., 1995), sultanas (Ka- rathanos & Belessiotis, 1997), and bananas (Maskan, 2000). Microwave heating resulted in greater increases in drying rates (Fig. 3), almost 13ą14 times higher com- pared to that with hot air drying at the start of the drying process. Data from the hot air, microwave and combined hot air-microwave drying were used to test the applicability of Eq. (1). The parameter k was evaluated using non- linear regression (Table 1) and the tness was illustrated in Fig. 1. The analysis yielded excellent t with high values of r2 for hot air drying (0.988) and microwave drying (0.997). On the other hand, the model did not t all the data of the combined drying method. Therefore, it was applied to the hot air and microwave sections separately. In this case, the r2 value were 0.999 for hot air section and 0.001 for microwave section which in- Fig. 3. Drying rate curves of kiwifruit slices under various conditions. dicated a very poor t for the latter. Shrinkage took place during drying by all the drying methods tested and it was calculated using Eq. (2). The also obtained with the microwave drying (Fig. 3) with eect of drying method on shrinkage of kiwifruits was no constant rate period. The rst falling rate period was shown in Fig. 4. The shrinkage of kiwifruit samples was from the beginning of drying to about 1.9 kg water/kg 85%, 81% and 76% for microwave, hot air and hot air- dry solids and was followed by a rapidly decreasing microwave drying, respectively. Hot air drying pro- second falling rate period. The reason for existence of moted a moderate shrinkage, which was explained by two falling rate periods may be due to case hardening the fact that a long drying time gives more time for the which acts as a barrier to moisture migration during product to shrink (Ratti, 1994). The shrinkage was the prolonged drying. The case hardening is because of the Table 1 Nonlinear regression analysis results of one parameter diusion model (Eq. (1)) for drying of kiwifruits Parameter Drying method Air Microwave Hot air-mircrowave drying drying drying Air section Microwave section k 0.0103 0.1798 0.0094 0.0208 SE ( ) 0.0002 0.0305 0.0001 0.0058 r2 0.988 0.997 0.999 0.0010 M. Maskan / Journal of Food Engineering 48 (2001) 177ą182 181 Fig. 4. Shrinkage of kiwifruit slices during drying. Fig. 5. Rehydration behaviour of dried kiwifruit slices at 50C. least by combined drying method. However, there was a showing that a less shrunk structure had higher capacity higher and rapid shrinkage of samples dried by micro- to absorb water when reconstituted. wave. It is because of extensive heat generation, accel- erating removal of water from the tissues in the sample by microwave. In all processes shrinkage followed the 4. Conclusion pattern of typical drying curves (Fig. 1), with high shrinkage initially and gradual levelling o towards the From the above results it was concluded that micro- end of drying so that the nal size and shape of samples were xed before drying was completed. Similar beha- wave and microwave assisted heating reduced the drying times by 89ą40%. The one-parameter diusion model viour has been observed by Ratti (1994) on drying of adequately described the hot air and microwave drying potatoes, apples and carrots, Sjoholm and Gekas (1995) on apple drying and Wang and Brennan (1995) on po- data. 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