8589356376

8589356376



L. Kozhitow A. Kostikoia. V. Kozlov. Zh. \fyrkhalvkov. A. Saipow FEATURES OFFeNi3 NANOPARTICLES IN POLYACRYLONITRILE FORMATION UNDERINFRARED HEATING

CONCLUSION

Thus the method of composite obtaining based on nanoparticles FeNi3 in the carbon materiał    from    the    system

FeCl3- 6H20/NiCl2- 6H20/P AN is developed under the infrared heating; the possibility of Fe and Ni reduction from metal chlorides by means of hydrogen emitted at temperaturę higher than 300°C under the polymer destruction is confirmed by the thcrmodynamic calculation. FeNi3 nanoparticle formation in the rangę from 20 to 60 nm is defined by X-ray phase analysis and using scanning electron microscopy.

REFERENCES

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Khomutov and G.Yu. Yurkov, 2005. Magnetic nanoparticles:    preparation, structure and

properties. Russian Chemical Reviews, 6(74): 489-520.

2.    Sun, S. and J.H. Zeng, 2002. Am. Size-Controlled Synthesis of Magnetite Nanoparticles. Chem. Soc, 124: 124-128.

3.    Bac, L.N., Y.S. Kwon and J.S. Kim. 2009. Synthesis and characteristic of FeNiintermetallic compound obtained by electrical explosion of wire. Materials Research Bulletin, 45: 352-354.

4.    Lu, X., G. Liang and Y. Zhang, 2007. Synthesis and characterization of magnetic FeNi3 particles obtained by hydrazine reduction in aąueous solution. Materiał Science and Engineering B, 139: 124-127.

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Journal of Industrial Technology and Engineering, 2012, 2(3): 5-10



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