000 011

Micromeritics Instrument Corporation




| Micromeritics Instrument Corporation


| Micromeritics Instrument Corporation




| Micromeritics Instrument Corporation






| Micromeritics Instrument Corporation












| Micromeritics Instrument Corporation






ASAP 2020C V2.00 G Unit 1 Serial #: 1309 Page 1

| ASAP 2020C V2.00 G Unit 1 Serial #: 1309 Page 1 | ASAP 2020C V2.00 G Unit 1 Serial #: 1309 Page 1

| ASAP 2020C V2.00 G Unit 1 Serial #: 1309 Page 1



| ASAP 2020C V2.00 G Unit 1 Serial #: 1309 Page 1









| ASAP 2020C V2.00 G Unit 1 Serial #: 1309 Page 1









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Sample: 5%Pd/SiO2 red. 300C



| Sample: 5%Pd/SiO2 red. 300C

| Sample: 5%Pd/SiO2 red. 300C



| Sample: 5%Pd/SiO2 red. 300C





| Sample: 5%Pd/SiO2 red. 300C











| Sample: 5%Pd/SiO2 red. 300C





Operator: MN



| Operator: MN

| Operator: MN



| Operator: MN





| Operator: MN











| Operator: MN





File: C:\...\PROF~1.KAR\000-011.SMP



| File: C:\...\PROF~1.KAR\000-011.SMP

| File: C:\...\PROF~1.KAR\000-011.SMP



| File: C:\...\PROF~1.KAR\000-011.SMP





| File: C:\...\PROF~1.KAR\000-011.SMP











| File: C:\...\PROF~1.KAR\000-011.SMP











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Started: 2011-01-25 17:46:14 Analysis Gas: CO

| Started: 2011-01-25 17:46:14 Analysis Gas: CO | Started: 2011-01-25 17:46:14 Analysis Gas: CO

| Started: 2011-01-25 17:46:14 Analysis Gas: CO



| Started: 2011-01-25 17:46:14 Analysis Gas: CO









| Started: 2011-01-25 17:46:14 Analysis Gas: CO



Completed: 2011-01-26 1:57:33 Analysis Temp: 35.0 °C

| Completed: 2011-01-26 1:57:33 Analysis Temp: 35.0 °C | Completed: 2011-01-26 1:57:33 Analysis Temp: 35.0 °C

| Completed: 2011-01-26 1:57:33 Analysis Temp: 35.0 °C



| Completed: 2011-01-26 1:57:33 Analysis Temp: 35.0 °C









| Completed: 2011-01-26 1:57:33 Analysis Temp: 35.0 °C



Report Time: 2011-03-17 10:59:11 Equilibration Interval: 10 s

| Report Time: 2011-03-17 10:59:11 Equilibration Interval: 10 s | Report Time: 2011-03-17 10:59:11 Equilibration Interval: 10 s

| Report Time: 2011-03-17 10:59:11 Equilibration Interval: 10 s



| Report Time: 2011-03-17 10:59:11 Equilibration Interval: 10 s









| Report Time: 2011-03-17 10:59:11 Equilibration Interval: 10 s



Sample Mass: 0.9928 g Low Pressure Dose: None

| Sample Mass: 0.9928 g Low Pressure Dose: None | Sample Mass: 0.9928 g Low Pressure Dose: None

| Sample Mass: 0.9928 g Low Pressure Dose: None



| Sample Mass: 0.9928 g Low Pressure Dose: None









| Sample Mass: 0.9928 g Low Pressure Dose: None



Entered free space: 16.1330 cm³ Automatic Degas: No

| Entered free space: 16.1330 cm³ Automatic Degas: No | Entered free space: 16.1330 cm³ Automatic Degas: No

| Entered free space: 16.1330 cm³ Automatic Degas: No



| Entered free space: 16.1330 cm³ Automatic Degas: No









| Entered free space: 16.1330 cm³ Automatic Degas: No









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Comments: Probka 1 dla prof. Karskiego




| Comments: Probka 1 dla prof. Karskiego


| Comments: Probka 1 dla prof. Karskiego




| Comments: Probka 1 dla prof. Karskiego






| Comments: Probka 1 dla prof. Karskiego












| Comments: Probka 1 dla prof. Karskiego












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Isotherm Tabular Report




| Isotherm Plot


| Analysis Summary




| Analysis Tabular Report






| Line Fit Plot












| Options Report






Analysis Data




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| Task Summary












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|

Element		 Percent
of Sample
Weight
(%)
Atomic
Weight
Stoichiometry
Factor		 Atomic
Cross-Sectional
Area
(nm²)

Density
(cm³/g)		 |
Pressure
(mmHg)		 Quantity
Adsorbed
(cm³/g STP)

Pressure
(mmHg)		 Quantity
Adsorbed
(cm³/g STP)

1st - Repeat
(cm³/g STP)
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Pressure
(mmHg)
Quantity
Adsorbed
(cm³/g STP)

Time
(hh:mm)
Repeat
Pressure
(mmHg)		 Repeat
Quantity
Adsorbed
(cm³/g STP)

Time
(hh:mm)		 | 5%Pd/SiO2 red. 300C - First analysis data point
5%Pd/SiO2 red. 300C - Repeat analysis data point
| palladium 5 106,4 1 0,0787 12,02 | 99,6400375366211 0,644007607136091
106,17414855957 0,199186574766121
0,444821032369969
| Selected first analysis data
Selected repeat analysis data
Difference


Non-selected first analysis data


Non-selected repeat analysis data
| Task
Number		 Task
Name
Gas		 Temp
(°C)		 Rate
(°C/min)		 Time
(min)		 Pressure
(mmHg)
99,6400375366211 0,644007607136091 00:28 106,17414855957 0,199186574766121 01:45 | Pressure (mmHg) Quantity Adsorbed (cm³/g STP) Pressure (mmHg) Quantity Adsorbed (cm³/g STP) |





| 156,682739257813 0,690356357552946 * 156,491912841797 0,239163426953704 * 0,451192930599242 * | Pressure (mmHg) Quantity Adsorbed (cm³/g STP) Pressure (mmHg) Quantity Adsorbed (cm³/g STP) Pressure (mmHg) Quantity Adsorbed (cm³/g STP) Pressure (mmHg) Quantity Adsorbed (cm³/g STP) Pressure (mmHg) Quantity Adsorbed (cm³/g STP) Pressure (mmHg) Quantity Adsorbed (cm³/g STP) Pressure (mmHg) Quantity Adsorbed (cm³/g STP) | 1 Evacuation He 300 10 60

156,682739257813 0,690356357552946 00:30 156,491912841797 0,239163426953704 01:47 | 99,6400375366211 0,644007607136091 106,17414855957 0,199186574766121 |





| 206,59162902832 0,727975247930473 * 206,654510498047 0,273873188693922 * 0,45410205923655 * | 156,682739257813 0,690356357552946 156,491912841797 0,239163426953704 156,682739257813 0,451192930599242 99,6400375366211 0,644007607136091 99,6400375366211 0,644007607136091 106,17414855957 0,199186574766121 106,17414855957 0,199186574766121 | 2 Flow H2 300 10 60

206,59162902832 0,727975247930473 00:32 206,654510498047 0,273873188693922 01:50 | 156,682739257813 0,690356357552946 156,491912841797 0,239163426953704 | Analysis Results




| 256,660552978516 0,763998437531451 * 256,343444824219 0,306565633615499 * 0,457432803915952 * | 206,59162902832 0,727975247930473 206,654510498047 0,273873188693922 206,59162902832 0,45410205923655 156,682739257813 0,690356357552946

156,491912841797 0,239163426953704

| 3 Evacuation
300 10 120

256,660552978516 0,763998437531451 00:34 256,343444824219 0,306565633615499 01:52 | 206,59162902832 0,727975247930473 206,654510498047 0,273873188693922 |





| 306,608367919922 0,799912830058176 * 306,450958251953 0,339244570490048 * 0,460668259568127 * | 256,660552978516 0,763998437531451 256,343444824219 0,306565633615499 256,660552978516 0,457432803915952 206,59162902832 0,727975247930473

206,654510498047 0,273873188693922

| 4 Evacuation
35 10 10

306,608367919922 0,799912830058176 00:37 306,450958251953 0,339244570490048 01:54 | 256,660552978516 0,763998437531451 256,343444824219 0,306565633615499 | Metal Dispersion: 5.5681 %



| 356,398590087891 0,83351443140373 * 356,541076660156 0,370215281471911 * 0,463299149931819 * | 306,608367919922 0,799912830058176 306,450958251953 0,339244570490048 306,608367919922 0,460668259568127 256,660552978516 0,763998437531451

256,343444824219 0,306565633615499

| 5 Leak Test
35 10


356,398590087891 0,83351443140373 00:39 356,541076660156 0,370215281471911 01:57 | 306,608367919922 0,799912830058176 306,450958251953 0,339244570490048 | Metallic Surface Area: 1.2403 m²/(g of sample)



| 406,35791015625 0,864865451840086 * 406,423522949219 0,400235035698643 * 0,464630416141443 * | 356,398590087891 0,83351443140373 356,541076660156 0,370215281471911 356,398590087891 0,46329914993182 306,608367919922 0,799912830058176

306,450958251953 0,339244570490048

| 6 Analysis CO 35 10


406,35791015625 0,864865451840086 00:41 406,423522949219 0,400235035698643 01:59 | 356,398590087891 0,83351443140373 356,541076660156 0,370215281471911 | Metallic Surface Area: 24.8059 m²/(g of metal)



| 456,440826416016 0,895441178617458 * 456,51171875 0,430801621334381 * 0,464639557283077 * | 406,35791015625 0,864865451840086 406,423522949219 0,400235035698643 406,35791015625 0,464630416141444 356,398590087891 0,83351443140373

356,541076660156 0,370215281471911

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456,440826416016 0,895441178617458 00:44 456,51171875 0,430801621334381 02:01 | 406,35791015625 0,864865451840086 406,423522949219 0,400235035698643 | Crystallite Size (6.000 V / A): 20.12296 nm



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| 456,440826416016 0,895441178617458 456,51171875 0,430801621334381 456,440826416016 0,464639557283077 406,35791015625 0,864865451840086

406,423522949219 0,400235035698643

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| 456,440826416016 0,895441178617458 456,51171875 0,430801621334381 | Y-Intercept Quantity Adsorbed: 0.5865 ± 0.0038 cm³/g STP



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456,440826416016 0,895441178617458

456,51171875 0,430801621334381

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| Slope: 0.000685 ± 0.000012



| * Included in calculation of line fit and difference data.






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| Correlation Coefficient: 9.99263E-01



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| Task Number: 6
















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| Adsorptive: Carbon Monoxide
















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| Temperature: 35.0 °C
















| Difference Results




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| Heat rate: 10.0 °C/min
















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| Equilibration interval: 10 s
















| Metal Dispersion: 4.2218 %



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| Relative target tolerance: 5.0 %
















| Metallic Surface Area: 0.9404 m²/(g of sample)



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| Absolute target tolerance: 5.000 mmHg
















| Metallic Surface Area: 18.8082 m²/(g of metal)



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| Crystallite Size (6.000 V / A): 26.53992 nm



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| Repeat analysis: Yes
















| Y-Intercept Quantity Adsorbed: 0.4447 ± 0.0017 cm³/g STP



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| Fast evacuation: No
















| Slope: 0.000048 ± 0.000005



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| Unrestricted evac. pressure: 30.0 mmHg
















| Correlation Coefficient: 9.72287E-01



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| Evacuation time: 30 min
















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| Free space group: Entered















































| Entered free space: 18.0000 cm³















































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| Incremental dosing: No















































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| Experiment Log
















































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| Task
Number		 Task
Name		 Start
Time
(h:min)
Gas		 Furnace
Temp.
(°C)		 Sample
Temp.
(°C)
Time
(min)
Pressure
(mmHg)










































| 1 EVAC 0:02 Hel 324 299,653045654297 60










































| 2 FLOW 1:54 H2 336 299,887115478516 60 747,510009765625










































| 3 EVAC 2:55
324 300,129364013672 120










































| 4 EVAC 5:13
31 34,1845321655273 10










































| 5 LEAK 6:05
30 33,4194564819336 1










































| 6 ANL 6:09 CO 34 34,681266784668 121 456,504455566406










































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| Leak Test Results
















































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|
Start Time
(min)		 Maximum Allowed
Outgas Rate
(µmHg/min)		 Observed
Outgas Rate
(µmHg/min)
Status













































| 369 50 1 Pass













































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