117828206

117828206



14


M. Sajewicz et al.

Table III. Dependence on the method of extractiona of the relative amountsb of volatile compounds isolated from samples of S. staminea collected in 2007 and 2008.

The retention times (*r) of the compounds are aiso given

Compound

fR (min)

Peak height (%)

HS-70

HS-80

Deryng

ASE

2007

2008

2007

2008

2007

2008

2007

2008

or-Pinene

10.97

10.09

3.72

8.75

5.28

2.64

6.36

Camphene

11.75

4.86

1.44

2.47

//-Pinene

12.20

5.23

6.47

5.39

11.50

3.05

0.11

/?-Myrcene

12.25

o-Cymene

13.15

Limonene

13.26

15.68

6.23

6.24

11.62

5.57

0.11

//-Phellandrene

13.32

/?-frans-Ocimene

13.36

3.93

Eucalyptol

13.50

3.58

3.88

1.12

5.85

0.54

4.47

ds-Ocimene

13.91

2.30

0.29

i-Terpinene

13.95

p-Mentha-1,4-

diene

14.59

Thujol

15.12

3.33

2.51

7.01

0.41

Thujenone

15.35

0.69°

1.64

1.49

0.30

Thujone

15.47

Camphor

16.11

Borneol

16.65

0.97

Bornyl acetale

18.84

/3-Chamigrene

21.60

2.98

6.44

|&2I

9.38

10.21

12.08

13.17

1211

Cadin-3,9-diene

22.43

1.41

3.49

2.19

4.60

6.30

6.39

4.70

3.90

Murolene

23.31

Isocaryophyllene

21.70

Caryophyllene

22.53

aHS-70, head-space extraction at 70°C; HS-80, head-space extraction at 80°C; Deryng, vapour distillation in a Deryng apparatus; ASE, accelerated solvent extraction bThe amount of a volatile compound extracted by a given method of extraction is expressed on the percentage scalę (as semi-quantitatively estimated from its respective peak height relative to the sum for all the volatile compounds)

cEmboldening indicates the chemotaxonomic advice compound (thujenone) estab-lished in previous work [14]



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