1. Slide the open end of the valve assembly over
the tapered tip of the Titret so that it fits snugly.
(Figure 1).
2. Snap the tip of the Titret by hand (Figure 2).
3. With the tip of the sample pipe immersed in the
sample, squeeze the bead valve briefly to pull in
a small amount of sample. CAUTION: Do not
squeeze the bead valve unless the sample pipe
is immersed below the surface of the liquid or
the vacuum will be lost and the test ruined.
(Figure 3).
4. Rock the Titret to mix the contents. The first
addition of sample will pull in the reagent from
the sample pipe. The contents of the ampoule
will turn a GREEN color.
5. Continue to add sample water until the liquid in
the Titret turns from GREEN to a bright
ORANGE.* When the orange color appears,
the end point has been reached. Stop test, hold
the Titret with its tip pointed upward and read the
scale opposite the liquid level. Check the con-
trol and dosage chart for the appropriate prod-
uct concentrations. (Figure 5)
*Note: Immediately before the end point is
reached, the contents will turn BLUE. Make
further additions with care.
PROCEDURE FOR USING THE TITRETTOR
2
1. Fill the sample cup to the 25ml mark with your
sample.
2. Push the valve assembly (in ampoule tray) onto
the Titret ampoule tip until it fits snugly (Figure 1).
3. Gently snap the tip of the ampoule at the score
mark (Figure 2).
4. Lift the control bar and insert the Titret assembly
into the body of the Titrettor (Figure 3).
5. With the tip of the sample pipe immersed in the
sample, press the control bar firmly, but briefly,
to pull in a small amount of sample (Figure 4).
CAUTION: If the control bar is pressed when
the sample pipe is not immersed in the liquid,
then the vacuum in the Titret will be destroyed.
6. Press the control bar again briefly to allow
another small amount of sample to be drawn into
the ampoule.
7. After each addition, rock the entire assembly to
mix the contents of the ampoule. Watch for the
color change from green to orange (end point).
8. Repeat steps 6 and 7 until the end point is
reached.
9. Remove the ampoule from the Titrettor. Hold
the Titret ampoule in a vertical position and
carefully read the test result on the scale oppo-
site the liquid level (Figure 5).
Printed in U.S.A.
©2001 Ashland Inc. ®Registered trademark,
TM
Trademark of Ashland Inc.
sm
Service Mark of Ashland Inc.
1
Registered trademark,
2
Trademark of CHEMetrics, Inc.
CW-CS-1 (1/01)R7
TEST RESULTS & DOSAGE REQUIREMENTS (Control Limits in Bold Italics)
CONVERSION CHART
MAXIGARD
®
diesel engine water treatment
SCALE
MAXIGARD
DOSAGE
UNITS
as ppm prod
in liters/tonne
Initial Dosage:
16.0 liters/tonne
1.0
12,000
*
6.0
1.1
13,000
6.0
1.2
14,000
6.0
1.3
16,000
6.0
1.4
17,000
4.0
1.5
18,000
4.0
1.6
19,000 Satisfactory - no dosage
1.8
22,000 Satisfactory - no dosage
2.0
24,000 Satisfactory - no dosage
2.5
30,000 Satisfactory - no dosage
3.0
36,000 Satisfactory - no dosage
3.5
42,000
High
4.0
48,000
High
Partially drain
5.0
60,000
High
and freshen
7.0
84,000
High
system
10.0
120,000
High
High quality distilled makeup water is recommended.
*
If readings are below 12,000 (scale unit 1.0), use 10.0 ltr/tonne and retest.
If system has been partially drained and refilled, use initial dosage.
CONVERSION CHART
DEWT
®
NC diesel engine water treatment
SCALE
DEWT NC
DOSAGE
UNITS
as ppm prod
in kgs/tonne
Initial Dosage:
3.2 kgs/tonne
1.0
800
2.7
1.1
900
2.7
1.2
1,000
2.3
1.3
1,100
2.3
1.4
1,200
2.3
1.5
1,300
2.3
1.6
1,400
2.3
1.8
1,500
1.8
2.0
1,700
1.8
2.5
2,200
1.4
3.0
2,600
0.9
3.5
3,000 Satisfactory - no dosage
4.0
3,400 Satisfactory - no dosage
5.0
4,300 Satisfactory - no dosage
7.0
6,000
High
10.0
8,600
High
High quality distilled makeup water is mandatory.
CONVERSION CHART
LIQUIDEWT
TM
cooling water treatment
SCALE
LIQUIDEWT
DOSAGE
UNITS
as ppm prod
in liters/tonne
Initial Dosage:
8.0 liters/tonne
1.0
8,000
*
1.5
1.1
9,000
1.5
1.2
10,000 Satisfactory - no dosage
1.3
11,000 Satisfactory - no dosage
1.4
12,000 Satisfactory - no dosage
1.5
13,000 Satisfactory - no dosage
1.6
14,000 Satisfactory - no dosage
1.8
15,000 Satisfactory - no dosage
2.0
17,000
High
2.5
22,000
High
3.0
26,000
High
Partially drain
3.5
30,000
High
and freshen
4.0
34,000
High
system
5.0
43,000
High
7.0
60,000
High
10.0
86,000
High
High quality distilled makeup water is recommended.
*
If readings are below 8,000 (scale unit 1.0), use 5.0 ltr/tonne and retest.
If system has been partially drained and refilled, use initial dosage.
Drew Marine Division
Valve
Assembly
Score
Mark
Reference
Line
Ampoule
1
Lift control bar
3
Watch for
color change
here.
Press
control bar
Sample
4
Sample pipe
COOLING WATER TREATMENT- TESTING, CONTROL AND DOSAGE CHART
CWT TITRET
1
TEST METHOD
For use with LIQUIDEWT
TM
cooling water treatment, MAXIGARD
®
diesel engine water treatment and DEWT
®
NC diesel engine water treatment
Apparatus: CWT Titrets Test Set Order No. 0367-01-2
PROCEDURE WITHOUT USING THE TITRETTOR
2
Snap the
tip at the
score mark
2
Read
scale units
when color
changes
permanently.
5
DREW
sm
Technical
Service
ALTERNATE TEST FOR DEWT
®
NC diesel engine water treatment
Preferred method is to use the CWT Titrets
1
Apparatus: DEWT NC Test Kit Order No. 0302-01-8
Test Kit Contains:
1
Cylinder, 50ml
Order No. 0236-01-9
1
0.2g spoon
Order No. 0224-01-4
1
DEWT NC Reagent No. 1, (100 gms) Order No. 0306-01-0
1
DEWT NC Reagent No. 2, (100 gms) Order No. 0307-01-8
PROCEDURE
1.
Draw a cooling water sample from a full flowing part of the system into the graduated mixing cylinder to the
25 ml mark. (Figure 1)
2.
Add 5 level measuring spoons of DEWT NC Reagent No. 1 and mix until all of the reagent is dissolved. (Figure 2)
3.
Add 1 level measuring spoon of DEWT NC Reagent No. 2, stopper the mixing cylinder, and thoroughly mix. (Figure 3)
4.
If the sample turns purple-red and the color lasts for at least 30 seconds, the test indicates that the treatment level
is below 500 ppm. However, if the color disappears within 30 seconds, add additional Reagent No. 2, one level measuring
spoon at a time (counting spoonfuls) with thorough mixing until the purple-red color persists for over 30 seconds.
5.
To determine the concentration of DEWT NC, count the total number of measuring spoons of Reagent No. 2 added
and convert to ppm.
Calculation: ppm DEWT NC = (number of spoons-1) x 500
6.
Record results as ppm DEWT NC on the Cooling Water Treatment Onboard Graphing Log (CW-LS-3).
7.
Determine the dosage of DEWT NC treatment required per tonne of circulating water as indicated on the Dosage Requirement Chart.
DOSAGE REQUIREMENT CHART (Control Limits in Bold Italics)
DEWT NC diesel engine water treatment
Total Number of
ppm
Measuring Spoons of
of DEWT NC
Dosage Requirement per Tonne
Reagent No. 2 Used
Recorded
of Circulating Water
1
None
3.2 kg (7 lbs.)
2
500
2.7 kg (6 lbs.)
3
1000
2.3 kg (5 lbs.)
4
1500
1.8 kg (4 lbs.)
5
2000
1.4 kg (3 lbs.)
6
2500
0.9 kg (2 lbs.)
7
3000
Satisfactory - No dose required.
8
3500
Satisfactory - No dose required.
9
4000
Satisfactory - No dose required.
10
4500
Satisfactory - No dose required.
11
5000
High - No dose required.
The use of high quality, distilled makeup water is recommended as the best means
of controlling scale formation for LIQUIDEWT
TM
and MAXIGARD
®
-treated systems
and is mandatory for DEWT NC-treated systems.
REFERENCE TESTS FOR MAKEUP WATER CONTAMINANTS
Use any one of the following parameters as an indicator of makeup water contamination.
Parameter
Limit
Conductivity
500
µ
mhos maximum
Chloride
100 ppm maximum
Hardness
170 ppm maximum
*If any parameter is higher than the maximum, use better quality water.
CHLORIDE SAMPLE PRETREATMENT
Use for cooling water treated with MAXIGARD or LIQUIDEWT treatments.
Apparatus and Reagents
Drew Chloride LMP Test Kit
PCN 0373-01-9
Sample Pretreatment 50 gm
PCN 0374-02-5
(includes 0.5 gm scoop)
Filter Paper, Box of 100
PCN 0225-01-2
Funnel, Plastic
PCN 0221-01-0
Stirring Rod, Plastic, 150mm
PCN 0417-01-5
PROCEDURE
1. Add one scoop (0.5 gm) of Sample Pretreatment to approximately 70 ml of cooling water and stir well.
2. Let stand for two (2) minutes to allow precipitate to settle.
3. Filter the sample and proceed with the chloride detemrination using the Drew Chloride LMP Test Kit.