Alkohol |
Pik |
H piku [mm] |
0,5 H piku [mm] |
W0,5 [mm] |
Pole |
Pole śr. Palk |
100% |
1 |
84 |
42,0 |
1,3 |
109,20 |
114,83 |
2 |
90 |
45,0 |
1,3 |
117,00 |
3 |
91 |
45,5 |
1,3 |
118,30 |
94% |
1 |
89 |
44,5 |
1,3 |
115,70 |
118,63 |
2 |
90 |
45,0 |
1,3 |
117,00 |
3 |
88 |
44,0 |
1,4 |
123,20 |
90% |
1 |
92 |
46,0 |
1,3 |
119,60 |
124,80 |
2 |
91 |
45,5 |
1,4 |
127,40 |
3 |
91 |
45,5 |
1,4 |
127,40 |
86% |
1 |
91 |
45,5 |
1,3 |
118,30 |
122,50 |
2 |
89 |
44,5 |
1,4 |
124,60 |
3 |
89 |
44,5 |
1,4 |
124,60 |
80% |
1 |
88 |
44,0 |
1,2 |
105,60 |
108,57 |
2 |
89 |
44,5 |
1,3 |
115,70 |
3 |
87 |
43,5 |
1,2 |
104,40 |
et3 |
1 |
84 |
42,0 |
1,3 |
109,20 |
115,67 |
2 |
86 |
43,0 |
1,3 |
111,80 |
3 |
90 |
45,0 |
1,4 |
126,00 |
et4 |
1 |
88 |
44,0 |
1,4 |
123,20 |
116,23 |
2 |
84 |
42,0 |
1,4 |
117,60 |
3 |
83 |
41,5 |
1,3 |
107,90 |
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Woda |
Pik |
H piku [mm] |
0,5 H piku [mm] |
W0,5 [mm] |
Pole |
Pole śr. Pwd. |
0% |
1 |
- |
- |
- |
- |
- |
2 |
- |
- |
- |
- |
3 |
- |
- |
- |
- |
6% |
1 |
18 |
9,0 |
1,5 |
27,00 |
29,00 |
2 |
20 |
10,0 |
1,5 |
30,00 |
3 |
20 |
10,0 |
1,5 |
30,00 |
10% |
1 |
33 |
16,5 |
1,4 |
46,20 |
47,13 |
2 |
34 |
17,0 |
1,4 |
47,60 |
3 |
34 |
17,0 |
1,4 |
47,60 |
14% |
1 |
48 |
24,0 |
1,7 |
81,60 |
82,17 |
2 |
48 |
24,0 |
1,7 |
81,60 |
3 |
49 |
24,5 |
1,7 |
83,30 |
20% |
1 |
59 |
29,5 |
2 |
118,00 |
120,00 |
2 |
61 |
30,5 |
2 |
122,00 |
3 |
60 |
30,0 |
2 |
120,00 |
et3 |
1 |
50 |
25,0 |
1,8 |
90,00 |
91,80 |
2 |
50 |
25,0 |
1,8 |
90,00 |
3 |
53 |
26,5 |
1,8 |
95,40 |
et4 |
1 |
64 |
32,0 |
2,1 |
134,40 |
137,27 |
2 |
65 |
32,5 |
2,2 |
143,00 |
3 |
64 |
32,0 |
2,1 |
134,40 |
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Próbka |
94 |
90 |
86 |
80 |
et3 |
et4 |
M |
12,32 |
7,08 |
4,83 |
3,15 |
3,42 |
2,40 |
P (P=Palk/Pwo) |
4,09 |
2,65 |
1,49 |
0,90 |
1,26 |
0,85 |
% wagowy etanolu |
94,0 |
90,0 |
86,0 |
80,0 |
81,3 |
75,3 |
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Obliczam M na podstawie wzoru |
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M=(ret.cp)/(rH2O(100-cp)) |
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r et = |
0,7851 |
g/ml |
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r H2O = |
0,9982 |
g/ml |
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Obliczam cp na podstawie wzoru: |
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cp = (100MrH20)/(ret + rH20M) |
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Tułaza Łukasz |
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17.05.2005 |
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TŻ. Gr7 nr11 |
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Ćwiczenie 9 |
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Chromatografia gazowa |
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